
Ball-milled 600 °C biochar/GCE had the smallest peak-to-peak separation, series resistance, and charge transfer resistance, implying its best electrocatalytic activity for the reduction of Fe (CN)63−, indicating potential application of the novel BM-biochar for low cost and high efficient electrodes. 20 View 1 excerpt, cites background
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Ball milling significantly modified the physicochemical properties of stover. The dramatic decrease of particle size leaded to a decrease of entanglement between particles, and the increase of free water enhanced the lubrication; these two factors significantly reduce the viscosity and yield stress of BMCS slurries.
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Abstract In this study, we employed microwave irradiation for activating boron concentrate, an abundant but low-grade boron mineral resource in China. The boron concentrate was pretreated by microwave irradiation based on TG-DTG-DSC analysis, and the influence of each parameter on processing efficiency was characterized using chemical analysis, XRD, SEM, FTIR and particle distribution analysis.
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Boron for liquid fuel Engines-A review on synthesis, dispersion stability in liquid fuel, and combustion aspects. Progress in Aerospace Sciences, Vol. 100. ... Physicochemical properties of ball milled boron particles: Dry vs. wet ball milling process. Powder Technology, Vol. 269.
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commercial 96% boron with strong crystalline phase and the same 96% boron (B) after ball milling. The effects of the properties of the starting B powder on the superconductivity were evaluated. We observed that samples using ball-milled 96% B, in comparison with the one made from the as-supplied 96% B, were character-
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Oct 23, 2020XrD and eDs were adopted to characterize the sea shell powder for its chemical constituents, particle size and secondary element formation.. mechanical properties like hardness and compressive...
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Citation: Wlodarski K, Tajber L, Sawicki W., Physicochemical properties of direct compression tablets with spray dried and ball milled solid dispersions of tadalafil in PVP-VA, European Journal of Pharmaceutics and Biopharmaceutics, 109, 2016, 14 - 23
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T1 - In vitro digestibility and physicochemical properties of milled rice. AU - Dhital, Sushil. AU - Dabit, Laura. AU - Zhang, Bin. AU - Flanagan, Bernadine. AU - Shrestha, Ashok K. PY - 2015/4/1. Y1 - 2015/4/1. N2 - Rice is a staple diet as well as a major ingredient in many processed foods. The physicochemical and supra-molecular structure of ...
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Ball-milling disrupted the layered structure of the h-BN, resulting in significant increases of surface area. Ball-milling at 400 rpm gave the highest surface area of 412 m 2 g -1 while higher rotation speeds decreased the surface areas due to agglomeration.
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Boron has been employed as an energetic material for ramjet solid additives and for solid propellants of ducted rockets because of its exceptionally high combustion enthalpy per unit volume [ 1, 2, 3 ]. Boron has also been used as a catalyst additive and support material [ 4, 5, 6, 7, 8, 9 ].
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Boron nitride nanosheets (BNNS) exfoliated by physical or chemical methods frequently exhibit poor dispersity in common solvents due to incomplete exfoliation and a low degree of functionalization, which has severely impacted BNNS application performances as polymer and lubricant additives. In this work, we mechanically exfoliated the bulk boron nitride into nanosheets through a ball-milling ...
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MgB2 samples were prepared using as-supplied commercial 96% boron with strong crystalline phase and the same 96% boron (B) after ball milling. The effects of the properties of the starting B powder on the superconductivity were evaluated. We observed that samples using ball-milled 96% B, in comparison with the one made from the as-supplied 96% ...
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A Universal Power Law Governing the Accuracy of Wave Function-Based Electronic Structure Calculations. Jerzy Cioslowski *. and. Krzysztof Strasburger. The Journal of Physical Chemistry Letters 2022, 13, 34, 8055-8061 (Physical Insights into Quantum Phenomena and Function) Publication Date (Web): August 22, 2022.
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Abstract: ${rm MgB}_{2}$ samples were prepared using as-supplied commercial 96% boron with strong crystalline phase and the same 96% boron (B) after ball milling. The effects of the properties of the starting B powder on the superconductivity were evaluated. We observed that samples using ball-milled 96% B, in comparison with the one made from the as-supplied 96% B, were characterized by ...
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Compositions, methods, and uses of aragonite biobased polymer plastic compositions are presented having increased strength and stiffness as well as improved recyclability and/or biodegradability. The aragonite biobased plastic compositions include aragonite blended in a dispersion with a biobased polymer and optionally includes a petroleum-based polymer and/or a compatibilizer.
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Conventionally aqueous solution of 1 M HNO3 and the required boric boron carbide is prepared by carbothermic or acid (solid) was added with constant stirring on hot magnesio-thermic reduction of boric acid or B2O3 [1]. plate. The contents were allowed to digest for 15 mins. There were in- depth studies on the carbothermic The white rubbery gel ...
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The Journal of Physical Chemistry C 2015, 119 (23), 13306-13313. ... Effects of post-thermal treatments of ball-milled boron nitrides on solid base catalysis. Catalysis Today 2020, 352, 279-286. ... Structural and physical properties of boron nitride nanotubes and their applications in nanocomposites. 2016,,, 183-199.
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Physicochemical properties of ball milled boron particles: Dry vs. wet ball milling process Powder Technology, Vol. 269 Thermal explosion synthesis of a magnesium diboride powder 21 November 2014 | Combustion, Explosion, and Shock Waves, Vol. 50, No. 6 Ignition, combustion, and oxidation of mixtures of amorphous and crystalline boron powders
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Both rotate speed and milling time affected the physicochemical properties and leaching process. • B 2 O 3 leaching rate would be enhanced with the increase of crystal amorphization and the decrease of chemical bonds stability. • Dehydroxylation after milling made it easier to absorb OH − from alkaline leaching solution. 1. Introduction
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The boron nitrides after evacuation gave moderate product yield for Knoevenagel condensation of benzaldehyde with malononitrile at 40 °C. The boron nitrides after calcination showed different...
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One-dimensional (1D) nanomaterials with novel photoelectric, magnetic, mechanical, and electronic transport properties have long been the research focus throughout the world. Herein, the recent achievements in preparation of 1D boron nitride nanomaterials, including nanotubes, nanowires, nanoribbons, nanorods, and nanofibres are reviewed. As the most intriguing and researched polymorph, boron ...
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Abstract—The structure and the physicochemical properties of boron carbide powders obtained by the mechanochemical synthesis of the carbon char and amorphous boron mix by applying the methods of the X-ray phase analysis (XPA), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and chemical analysis were investigated.On the basis of the X-ray phase analysis, it was ...
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Nov 26, 2018 The effect of ball milling on physicochemical, functional and rheological properties and structural characteristics of cold-extruded whey protein isolate (TWPI) was investigated as a function of grinding time. ... Hexagonal boron nitride (h-BN) was ball-milled at various rotation speeds (150-600 rpm) using a planetary ball-mill. ...
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A ball-milling system provides the kinetic energy for reducing the material into small fragments. Besides, the involved energy may start chemical reactions, paving the way for fast organic...
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Boron nitride (BN) nanomaterials have been increasingly explored for potential applications in chemistry and biology fields (e.g., biomedical, pharmaceutical, and energy industries) due to their unique physico-chemical properties. However, their safe utilization requires a profound knowledge on their potential toxicological and environmental impact. To date, BN nanoparticles have been ...
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Ball-milled sulfur-doped graphene materials contain metallic impurities originating from ball-milling apparatus: their influence on the catalytic properties. Chun Kiang Chua Division of Chemistry and Biological Chemistry, School of Physical and Mathematical Sciences, Nanyang Technological University, Singapore 637371, Singapore.
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In this paper, effects of ball-milled roasted chickpea (RC) powder on yogurt physiochemical, rheological, and sensorial properties were investigated. It was revealed that the addition of powder caused a gradual decline in pH values of pre-inoculated samples with corresponding increases in powder concentration from 1 to 5 g/ 100 mL.
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Abstract Hexagonal boron nitride (h-BN) was ball-milled at various rotation speeds (150-600 rpm) using a planetary ball-mill. Ball-milling disrupted the layered structure of the h-BN, resulting in significant increases of surface area.
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Ball milling is an effective method to reduce the boron particle size, so, the effects of ball milling boron powders in different media, such as acetone, ethanol, and toluene, on the superconducting properties of MgB2 needed to be considered and studied. It was observed that toluene was the most effective medium of them all for enhancing Jc.
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The U.S. Department of Energy's Office of Scientific and Technical Information
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Nov 20, 2021Boron nitride nanosheets (BNNS) exfoliated by physical or chemical methods frequently exhibit poor dispersity in common solvents due to incomplete exfoliation and a low degree of functionalization, which has severely impacted BNNS application performances as polymer and lubricant additives. In this work, we mechanically exfoliated the bulk boron nitride into nanosheets through a ball-milling ...
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The purpose of this study was to investigate the effect of working volume in the high-energy ball-milling process on the breakage characteristics (i.e., particle size, morphology, and chemical composition) and adsorption performance of rice straw ash. This study was conducted to confirm working volume issue since this parameter has correlations with the scaling-up process, the amount of input ...
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Jan 6, 2021Nilssen BE, Kleiv RA (2020) Silicon powder properties produced in a planetary ball mill as a function of grinding time, grinding ... (2015) Physicochemical properties of ball milled boron particles: Dry vs. wet ball milling process. Powder Technol 269:548-553. ... Ali ME et al (2013) Surfactant assisted ball milling: a simple top down ...
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3.Functionalisation of graphene. Owing to its unique morphology and exclusive properties, graphene has been demonstrated as an attractive candidate for batteries, but it is rare for graphene-based electrodes with desirable characteristics to also have essential surface properties specific for certain applications [].In several cases, functionalisation is the ideal approach to realise the ...
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Shoichiro Namba, Atsushi Takagaki, Keiko Jimura, Shigenobu Hayashi, Ryuji Kikuchi, S. Ted Oyama, Effects of ball-milling treatment on physicochemical properties and solid base activity of hexagonal boron nitrides, CATALYSIS SCIENCE & TECHNOLOGY, 10.1039/c8cy00940f, 9, 2, 302-309, 2019.01, Hexagonal boron nitride (h-BN) was ball-milled at ...
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The ball-milled boron nitrides were heated in a vacuum or air and used for Knoevenagel condensation. ... and X-ray photoelectron spectroscopy indicated that the heat treatment under vacuum hardly changed the physicochemical properties including crystal structure and surface composition whereas the heat treatment in air significantly altered the ...
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28 May 2015 | The Journal of Physical Chemistry A, Vol. 119, No. 24. Physicochemical properties of ball milled boron particles: Dry vs. wet ball milling process. Powder Technology, Vol. 269. Nanocomposite and mechanically alloyed reactive materials as energetic additives in chemical oxygen generators.
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ball-milled B are presented in comparison with the reference sample. II. EXPERIMENTAL DETAILS. MgB. 2. pellets were prepared by an. in situ. reaction pro-cess. B powder 96 % with strong crystalline phase was pre-pared by ball milling, with toluene as the ball-milling me-dium. The ball-milling process was carried out for 4, 8, and 12 h at a ...
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Five zirconia balls, each with diameter of 5 mm and mass of 0.4 g, were used for milling purpose. Weighing balance, having accuracy of 0.001 g, was used to weigh barium oxide and titanium oxide powders. Nano-ball milling was performed at 3000 rpm for 2 h.
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To test modified M-B-86 and M-B-95 powders suitability as precursor, MgB 2 samples were synthesized and characterized by means of powder x-ray diffraction (PXRD), scanning electron microscopy (SEM), transport measurements, Raman and EPR spectroscopy. In the following, we will discuss and comment on the results in context with the previously reported data for MgB 2 specimen prepared from the ...
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